中国药业
中國藥業
중국약업
China Pharmaceuticals
2015年
19期
44-44,45
,共2页
王争%王曙东%刘文雅%任海祥
王爭%王曙東%劉文雅%任海祥
왕쟁%왕서동%류문아%임해상
通塞益脑口服液%高效液相色谱法%α-细辛脑
通塞益腦口服液%高效液相色譜法%α-細辛腦
통새익뇌구복액%고효액상색보법%α-세신뇌
Tongsaiyinao Oral Solution%HPLC%α-asarone
目的:建立测定通塞益脑口服液中石菖蒲所含α-细辛脑含量的高效液相色谱法。方法色谱柱为 Hedera-ODS-2 C18柱(250 mm ×4.6 mm,5μm),流动相为甲醇-水(55:45),检测波长257 nm。结果α-细辛脑质量浓度在10.5~105μg/mL范围内与峰面积积分值线性关系良好( r=0.9999),平均加样回收率为99.49%,RSD为2.45%( n=6)。结论该方法简便、快速、重复性好,分离度好,测定结果准确可靠,可用于通塞益脑口服液中α-细辛脑的含量测定。
目的:建立測定通塞益腦口服液中石菖蒲所含α-細辛腦含量的高效液相色譜法。方法色譜柱為 Hedera-ODS-2 C18柱(250 mm ×4.6 mm,5μm),流動相為甲醇-水(55:45),檢測波長257 nm。結果α-細辛腦質量濃度在10.5~105μg/mL範圍內與峰麵積積分值線性關繫良好( r=0.9999),平均加樣迴收率為99.49%,RSD為2.45%( n=6)。結論該方法簡便、快速、重複性好,分離度好,測定結果準確可靠,可用于通塞益腦口服液中α-細辛腦的含量測定。
목적:건립측정통새익뇌구복액중석창포소함α-세신뇌함량적고효액상색보법。방법색보주위 Hedera-ODS-2 C18주(250 mm ×4.6 mm,5μm),류동상위갑순-수(55:45),검측파장257 nm。결과α-세신뇌질량농도재10.5~105μg/mL범위내여봉면적적분치선성관계량호( r=0.9999),평균가양회수솔위99.49%,RSD위2.45%( n=6)。결론해방법간편、쾌속、중복성호,분리도호,측정결과준학가고,가용우통새익뇌구복액중α-세신뇌적함량측정。
Objective To establish a method for the content determination of α-asarone in Tongsaiyinao Oral Solution. Methods The Hedera-ODS-2 C18 culumn ( 250 mm × 4. 6mm, 5 μm)column was used. The mobile phases consisted of methanol and water ( 55:45 ) and the detection wavelength was at 257 nm. Results α-asarone showed a linear relationship within the concentration range of 10. 5~105 μg/mL ( r=0. 999 9 ) . The average recovery was 99. 49%, and RSD=2. 45% ( n=6 ) . Conclusion The proposed method appered to be simple, rapid, reliable, sensitive and accurate. It is available to the content determination of Tongsaiyinao Oral Solution.