当代化工
噹代化工
당대화공
Contemporary Chemical Industry
2015年
10期
2300-2302
,共3页
邰石君%盛东海%杨君%罗根祥%李丽华%张金生
邰石君%盛東海%楊君%囉根祥%李麗華%張金生
태석군%성동해%양군%라근상%리려화%장금생
金属-有机骨架%微流控%纳米颗粒
金屬-有機骨架%微流控%納米顆粒
금속-유궤골가%미류공%납미과립
Metal-oganic framework%Continuous flow microreactor%Nano partical
利用微流控合成法，通过改变停留时间的方法，成功合成了尺寸可控的纳米金属-有机骨架nano-UiO 66。并将微流控合成产物与传统的反应釜合成产物进行比较，所有的产物均通过 X 射线粉末衍射、热重分析、扫描电镜表征其性质。
利用微流控閤成法，通過改變停留時間的方法，成功閤成瞭呎吋可控的納米金屬-有機骨架nano-UiO 66。併將微流控閤成產物與傳統的反應釜閤成產物進行比較，所有的產物均通過 X 射線粉末衍射、熱重分析、掃描電鏡錶徵其性質。
이용미류공합성법，통과개변정류시간적방법，성공합성료척촌가공적납미금속-유궤골가nano-UiO 66。병장미류공합성산물여전통적반응부합성산물진행비교，소유적산물균통과 X 사선분말연사、열중분석、소묘전경표정기성질。
Nano-sized UiO-66 (nano-UiO-66) particles were prepared in a continuous flow microreactor, in which the particle size can be tuned from hundreds to dozens of nanometers by changing the residence time. Then the products respectively prepared by continuous flow method and reaction kettle method were compared. All the products were characterized by PXRD, TGA and SEM.
