北方药学
北方藥學
북방약학
Journal of North Pharmacy
2015年
11期
1-1,2
,共2页
跌打祛风膏%质量标准%薄层色谱法
跌打祛風膏%質量標準%薄層色譜法
질타거풍고%질량표준%박층색보법
Diedaqufeng Cataplasm%Quality standard%TLC
目的:建立跌打祛风膏的质量标准。方法:采用薄层色谱法鉴别处方中大黄、薄荷脑等药材,并对乌头碱、士的宁做毒性限量检查。结果:大黄、薄荷脑的薄层色谱斑点清晰,分离度好,阴性无干扰;乌头碱、士的宁的毒性限量检查符合规定。结论:该实验方法操作简便,专属性强,重现性好,耐用性良好,结果准确可靠,可用于控制跌打祛风膏的质量。
目的:建立跌打祛風膏的質量標準。方法:採用薄層色譜法鑒彆處方中大黃、薄荷腦等藥材,併對烏頭堿、士的寧做毒性限量檢查。結果:大黃、薄荷腦的薄層色譜斑點清晰,分離度好,陰性無榦擾;烏頭堿、士的寧的毒性限量檢查符閤規定。結論:該實驗方法操作簡便,專屬性彊,重現性好,耐用性良好,結果準確可靠,可用于控製跌打祛風膏的質量。
목적:건립질타거풍고적질량표준。방법:채용박층색보법감별처방중대황、박하뇌등약재,병대오두감、사적저주독성한량검사。결과:대황、박하뇌적박층색보반점청석,분리도호,음성무간우;오두감、사적저적독성한량검사부합규정。결론:해실험방법조작간편,전속성강,중현성호,내용성량호,결과준학가고,가용우공제질타거풍고적질량。
Objective:To establish quality standard of Diedaqufeng Cataplasm. Mehtods:TLC method was used to distinguish rhubarb, menthol, and the toxicity of aconitine, strychnine set limit to test. Results:The spots of rhubarb and menthol were clear,good separating degree,negative without interference; the toxicity of aconitine and strychnine set limit to test compliance. Conclusion:The method is simple,exclusive,good reproducibility,durability ,accurate,and can be used for the quality control of Diedaqufeng Cataplasm.