通化师范学院学报
通化師範學院學報
통화사범학원학보
Journal of Tonghua Normal University
2015年
10期
43-45
,共3页
张小龙%李佳%姜雨虹%刘洋%王雅新
張小龍%李佳%薑雨虹%劉洋%王雅新
장소룡%리가%강우홍%류양%왕아신
CoPt%Au%溶胶-凝胶%磁性%尺寸
CoPt%Au%溶膠-凝膠%磁性%呎吋
CoPt%Au%용효-응효%자성%척촌
CoPt%Au%sol-gel%magnetism%size
利用溶胶-凝胶法制备CoPt, CoPt-Au纳米颗粒.并对制备的样品( CoPt, CoPt-Au纳米颗粒)的结构、形貌以及磁学性能进行了表征. X 射线衍射(XRD)结果表明,700°C时,CoPt, CoPt-Au纳米颗粒均为面心四方结构(FCT)的L10 相.透射电子显微镜( TEM)结果表明,CoPt较CoPt-Au的颗粒尺寸小,说明了Au掺杂可能促进了CoPt纳米颗粒的尺寸生长.振动样品磁强计( VSM)结果显示,CoPt-Au较CoPt的矫顽力大,说明一定量的Au元素掺杂可以促进CoPt纳米颗粒磁性的增长.
利用溶膠-凝膠法製備CoPt, CoPt-Au納米顆粒.併對製備的樣品( CoPt, CoPt-Au納米顆粒)的結構、形貌以及磁學性能進行瞭錶徵. X 射線衍射(XRD)結果錶明,700°C時,CoPt, CoPt-Au納米顆粒均為麵心四方結構(FCT)的L10 相.透射電子顯微鏡( TEM)結果錶明,CoPt較CoPt-Au的顆粒呎吋小,說明瞭Au摻雜可能促進瞭CoPt納米顆粒的呎吋生長.振動樣品磁彊計( VSM)結果顯示,CoPt-Au較CoPt的矯頑力大,說明一定量的Au元素摻雜可以促進CoPt納米顆粒磁性的增長.
이용용효-응효법제비CoPt, CoPt-Au납미과립.병대제비적양품( CoPt, CoPt-Au납미과립)적결구、형모이급자학성능진행료표정. X 사선연사(XRD)결과표명,700°C시,CoPt, CoPt-Au납미과립균위면심사방결구(FCT)적L10 상.투사전자현미경( TEM)결과표명,CoPt교CoPt-Au적과립척촌소,설명료Au참잡가능촉진료CoPt납미과립적척촌생장.진동양품자강계( VSM)결과현시,CoPt-Au교CoPt적교완력대,설명일정량적Au원소참잡가이촉진CoPt납미과립자성적증장.
CoPt and CoPt-Au nanoparticles are fabricated by Sol-gel method. Structure,morphology and magnetic properties of CoPt,CoPt-Au were characterized. X-ray diffraction ( XRD) results show that CoPt,CoPt-Au were faced centered tetragonal structure( FCT) at 700℃. Transmission electron microscopy ( TEM) results indicate that the CoPt-Au nano-particle has the larger size than CoPt. It means that Au could promote the growth of CoPt nanoparticles. The result of vibrating sample magnetometer ( VSM) indicates that the pure CoPt nanoparticles has the smaller coercivity than CoPt-Au nanoparticles. It indicates that the addition of Au could improve the magnetism of CoPt nanoparticles.