CAJ | 학술논문

利用非晶态Ru催化剂对间苯三酚进行加氢还原制备1,3,5-三羟基环己烷，并对加氢工艺的氢压、反应温度、反应时间、催化剂用量对产率的影响进行了探索。结果表明，温度为140℃，氢压为4MPa，催化剂的最佳用量为底物的1.5%，反应时间为12h时，1,3,5-三羟基环己烷的产率可达80%。
이용비정태Ru최화제대간분삼분진행가경환원제비1,3,5-삼간기배기완，병대가경공예적경압、반응온도、반응시간、최화제용량대산솔적영향진행료탐색。결과표명，온도위140℃，경압위4MPa，최화제적최가용량위저물적1.5%，반응시간위12h시，1,3,5-삼간기배기완적산솔가체80%。
1,3,5-cyclohexanetriol was synthesized by the amorphous Ru catalyst hydrogenation of m-trihydroxybenzene, the effect of pressure, temperature and the amount of catalyst on yield were also investigated. The results suggested that the yield of 1,3,5-Cyclohexanetriol was 80% when the temperature was 140℃,the pressure was 4MPa,the optimum dosage of the catalyst was 1.5% of the substrate, and the reaction time was 12h.