食品与药品
食品與藥品
식품여약품
Food and Drug
2015年
5期
360-363
,共4页
蔡桂萍%司徒伟良%宋粉云%钟兆健
蔡桂萍%司徒偉良%宋粉雲%鐘兆健
채계평%사도위량%송분운%종조건
橘红化痰丸%苦杏仁苷%反相高效液相色谱法%含量测定
橘紅化痰汍%苦杏仁苷%反相高效液相色譜法%含量測定
귤홍화담환%고행인감%반상고효액상색보법%함량측정
Juhong Huatan Wan%amygdalin%RP-HPLC%assay
目的建立反相高效液相色谱法(RP-HPLC)测定橘红化痰丸中苦杏仁苷含量的方法。方法色谱柱为Diamonsil C18;流动相为甲醇-0.1%磷酸水溶液(20:80),流速1.0 mL/min;检测波长210 nm;柱温30℃。结果苦杏仁苷在5.5~44.0μg/mL范围内有良好的线性关系(r=0.9991),平均回收率为100.3%,RSD为0.84%(n=6)。结论该法可用于橘红化痰丸中苦杏仁苷的含量测定。
目的建立反相高效液相色譜法(RP-HPLC)測定橘紅化痰汍中苦杏仁苷含量的方法。方法色譜柱為Diamonsil C18;流動相為甲醇-0.1%燐痠水溶液(20:80),流速1.0 mL/min;檢測波長210 nm;柱溫30℃。結果苦杏仁苷在5.5~44.0μg/mL範圍內有良好的線性關繫(r=0.9991),平均迴收率為100.3%,RSD為0.84%(n=6)。結論該法可用于橘紅化痰汍中苦杏仁苷的含量測定。
목적건립반상고효액상색보법(RP-HPLC)측정귤홍화담환중고행인감함량적방법。방법색보주위Diamonsil C18;류동상위갑순-0.1%린산수용액(20:80),류속1.0 mL/min;검측파장210 nm;주온30℃。결과고행인감재5.5~44.0μg/mL범위내유량호적선성관계(r=0.9991),평균회수솔위100.3%,RSD위0.84%(n=6)。결론해법가용우귤홍화담환중고행인감적함량측정。
Objective To establish a method for determination of amygdalin in Juhong Huatan Wan.MethodsA RP-HPLC method was established. The chromatographic column was Diamonsil C18. The mobile phase was a mixture of methanol-0.1 % phosphoric acid (20:80,v/v). The flow rate was 1.0 mL/min, and the detection wavelength was 210 nm. The column temperature was 30℃. ResultsThe linear range of amygdalin was 5.5-44.0μg/mL (r=0.9991). The average recovery for amygdalin was 100.3 %,withRSD of 0.84 % (n=6).Conclusion This method can be used for quantitative determination of amygdalin in the preparation.