CAJ | 학술논문

文章通过对水产品中孔雀石绿、隐性孔雀石绿及己烯雌酚的测定研究，优化了孔雀石绿、隐性孔雀石绿及己烯雌酚的质谱条件，并建立了同时测定水产品中这三种物质的高效液相色谱－串联质谱检测方法。利用此方法分析时间较短，且灵敏度高，回收率和重现性等均能满足定量分析要求，结果准确可靠。适于水产品中孔雀石绿、隐性孔雀石绿及己烯雌酚标准物质的同时测定，尤其适合大批量样品快速准确的定性定量分析。
문장통과대수산품중공작석록、은성공작석록급기희자분적측정연구，우화료공작석록、은성공작석록급기희자분적질보조건，병건립료동시측정수산품중저삼충물질적고효액상색보－천련질보검측방법。이용차방법분석시간교단，차령민도고，회수솔화중현성등균능만족정량분석요구，결과준학가고。괄우수산품중공작석록、은성공작석록급기희자분표준물질적동시측정，우기괄합대비량양품쾌속준학적정성정량분석。
The mass spectrometry param eters for determine diethylstilbestrol, malachite green, leumalachite green was optimized and a high-performance liquid chromatography-mass spectrometry method was established for the determination of three compounds. The results showed that such a method had the advantages of time-saving, with high sensitivity and accuracy, and it was suitable for quantitative analysis of diethylstilbestrol, malachite green, leumalachite green at same time, especially suitable for large quantities of samples.