中国中医药信息杂志
中國中醫藥信息雜誌
중국중의약신식잡지
Chinese Journal of Information on Traditional Chinese Medicine
2015年
11期
82-85
,共4页
张平%黄聪琳%张明童%杨静%王晓琳
張平%黃聰琳%張明童%楊靜%王曉琳
장평%황총림%장명동%양정%왕효림
红芪%薄层色谱%芒柄花素%高效液相色谱法%特征图谱
紅芪%薄層色譜%芒柄花素%高效液相色譜法%特徵圖譜
홍기%박층색보%망병화소%고효액상색보법%특정도보
Hedysari Radix%TLC%formononetin%HPLC%characteristic spectrum
目的 研究红芪药典标准,优化红芪药材的质量标准.方法 从性状、薄层色谱鉴别、高效液相色谱(HPLC)测定、水分、总灰分、醇溶性浸出物等方面对8批红芪药材质量标准进行研究.结果 红芪药材性状描述有别于以往文献记载,薄层色谱鉴别采用乙酸乙酯-三氯甲烷-水(4:9:1)展开系统,效果优于 2010 年版《中华人民共和国药典》红芪标准.以芒柄花素为对照,建立了红芪HPLC特征图谱.结论 本研究所建立的红芪薄层鉴别方法简单易行、准确可靠.
目的 研究紅芪藥典標準,優化紅芪藥材的質量標準.方法 從性狀、薄層色譜鑒彆、高效液相色譜(HPLC)測定、水分、總灰分、醇溶性浸齣物等方麵對8批紅芪藥材質量標準進行研究.結果 紅芪藥材性狀描述有彆于以往文獻記載,薄層色譜鑒彆採用乙痠乙酯-三氯甲烷-水(4:9:1)展開繫統,效果優于 2010 年版《中華人民共和國藥典》紅芪標準.以芒柄花素為對照,建立瞭紅芪HPLC特徵圖譜.結論 本研究所建立的紅芪薄層鑒彆方法簡單易行、準確可靠.
목적 연구홍기약전표준,우화홍기약재적질량표준.방법 종성상、박층색보감별、고효액상색보(HPLC)측정、수분、총회분、순용성침출물등방면대8비홍기약재질량표준진행연구.결과 홍기약재성상묘술유별우이왕문헌기재,박층색보감별채용을산을지-삼록갑완-수(4:9:1)전개계통,효과우우 2010 년판《중화인민공화국약전》홍기표준.이망병화소위대조,건립료홍기HPLC특정도보.결론 본연구소건립적홍기박층감별방법간단역행、준학가고.
Objective To study the pharmacopoeia standards of Hedysari Radix;To optimize the quality standards of Hedysari Radix medicinal materials.Methods Quality standards of eight batches of Hedysari Radix medicinal materials were studied from the aspects of properties, TLC identification, HPLC determination, the content of water and total ash, alcohol soluble extract, etc. Results The property description was different from the previous literature. The effects of TLC identification using ethyl acetate-chloroform-water (4:9:1) system is better than the standards in 2010 edition of Chinese Pharmacopoeia. With formononetin as reference, the HPLC characteristic spectrum of Hedysari Radix was established.Conclusion The TLC identification method is simple, accurate and reliable.
