CAJ | 학술논문

目的：建立宣肺清热合剂的质量标准。方法采用薄层色谱法对宣肺清热合剂中枳壳和桑白皮进行定性鉴别，采用高效液相色谱法对制剂中黄芩苷进行定量鉴别。结果枳壳和桑白皮的薄层色谱鉴别方法专属性强。黄芩苷进样质量的线性范围为0.032~2.59μg(r=0.9996)，回收率为100.08%(RSD=1.6%)。结论建立的方法定性专属性强、定量准确度高，适用于宣肺清热合剂的质量控制。
목적：건립선폐청열합제적질량표준。방법채용박층색보법대선폐청열합제중지각화상백피진행정성감별，채용고효액상색보법대제제중황금감진행정량감별。결과지각화상백피적박층색보감별방법전속성강。황금감진양질량적선성범위위0.032~2.59μg(r=0.9996)，회수솔위100.08%(RSD=1.6%)。결론건립적방법정성전속성강、정량준학도고，괄용우선폐청열합제적질량공제。
Objective To establish quality standard of Xuanfeiqingre mixture. Methods TLC was used to qualitatively identify Fructus Aurantii and Cortex Mori in Xuanfeiqingre mixture, and HPLC method was used to quantitatively iden-tify baicalin in mixture. Results TLC identification for Fructus Aurantii and Cortex Mori was specific and distinct. Baicalin showed a good liner relationship within the range from 0.032μg to 2.59μg (r=0.9996), the average recovery was 100.08%, with RSD of 1.6%. Conclusion This established method is qualitatively exclusive and quantitatively ac-curate, which is suitable for quality control of Xuanfeiqingre mixture.