CAJ | 학술논문

用薄层色谱/氢火焰离子化检测器（TLC/FID）和气相色谱-质谱联用（GC-MS）分别快速检测橡胶油的多环芳香族化合物（PCA）和多环芳烃（PAHs）含量。结果表明：TLC/FID与IP 346检测的橡胶油PCA含量接近，TLC/FID检测法的加标回收率为95%~105%；GC-MS与德国BIU公司检测的橡胶油PAHs含量接近， GC-MS检测法的加标回收率为97%~104%。2种检测方法操作简单、试剂用量小、准确度高、重复性好。
용박층색보/경화염리자화검측기（TLC/FID）화기상색보-질보련용（GC-MS）분별쾌속검측상효유적다배방향족화합물（PCA）화다배방경（PAHs）함량。결과표명：TLC/FID여IP 346검측적상효유PCA함량접근，TLC/FID검측법적가표회수솔위95%~105%；GC-MS여덕국BIU공사검측적상효유PAHs함량접근， GC-MS검측법적가표회수솔위97%~104%。2충검측방법조작간단、시제용량소、준학도고、중복성호。
The PCA and PAHs contents in rubber oil were measured rapidly by TLC/FID and GC-MS, respectively. The experimental testing results showed that the PCAs content of rubber oil measured by TLC/FID was close to the IP 346 method, while the recovery of added standard was 95%~105% by using TLC/FID. The PAHs content of rubber oil detected by GC-MS was close to the result measured by German company BIU, and the recovery of added standard was 97%~104% with GC-MS method. These two detection methods are simple, consume only small amount of testing reagents, and provide high accuracy and good reproducibility.