食品研究与开发
食品研究與開髮
식품연구여개발
Food Research and Development
2015年
20期
96-99
,共4页
柚皮精油%超临界流体萃取%响应面分析
柚皮精油%超臨界流體萃取%響應麵分析
유피정유%초림계류체췌취%향응면분석
pomelo skin oil%supercritical fluid extraction%response surface methodology
以平和琯溪蜜柚柚皮为原材料,运用响应面法优化超临界CO2萃取技术提取柚皮精油。根据BOX (Box-Benhnken)试验设计原理,确定萃取压力、萃取温度、萃取时间及二氧化碳流量对精油萃取率的影响。结果表明:超临界二氧化碳萃取柚皮精油的最佳工艺条件为萃取温度为59.97℃、萃取压力为25 MPa、萃取时间为150 min、二氧化碳流量为15 L/h,在此萃取条件下,柚皮香精油的萃取出油率为5.62%。
以平和琯溪蜜柚柚皮為原材料,運用響應麵法優化超臨界CO2萃取技術提取柚皮精油。根據BOX (Box-Benhnken)試驗設計原理,確定萃取壓力、萃取溫度、萃取時間及二氧化碳流量對精油萃取率的影響。結果錶明:超臨界二氧化碳萃取柚皮精油的最佳工藝條件為萃取溫度為59.97℃、萃取壓力為25 MPa、萃取時間為150 min、二氧化碳流量為15 L/h,在此萃取條件下,柚皮香精油的萃取齣油率為5.62%。
이평화관계밀유유피위원재료,운용향응면법우화초림계CO2췌취기술제취유피정유。근거BOX (Box-Benhnken)시험설계원리,학정췌취압력、췌취온도、췌취시간급이양화탄류량대정유췌취솔적영향。결과표명:초림계이양화탄췌취유피정유적최가공예조건위췌취온도위59.97℃、췌취압력위25 MPa、췌취시간위150 min、이양화탄류량위15 L/h,재차췌취조건하,유피향정유적췌취출유솔위5.62%。
The production of naringin of Guanxi honey pomelo , used carbon dioxide as a medium by supercritical fluid extraction technology to pomelo peel essential oil from pomelo skin , response surface methodology(RSM) was employed to optimize the extraction. According to the principle of Box-Behnken central composite design, extraction pressure, extraction temperature, extraction time and carbon dioxide flow rate were chosen as response factors, extraction mass as response value, and a four-factor and three levels central composite design was adopted to determine the influence of various technological conditions. The results showed that better extraction conditions were 59.97℃of temperature, 25 MPa of extracting pressure,150min of period, 15 L/h of CO2 flow rate. Under these conditions, the yield of pomelo skin oil was 5.62%.