食品研究与开发
食品研究與開髮
식품연구여개발
Food Research and Development
2015年
20期
137-140
,共4页
窦文渊%黄腾花%黄名湖%许慧鹊
竇文淵%黃騰花%黃名湖%許慧鵲
두문연%황등화%황명호%허혜작
电感耦合等离子发射光谱%桑树%检测%元素
電感耦閤等離子髮射光譜%桑樹%檢測%元素
전감우합등리자발사광보%상수%검측%원소
ICP-AES%mulberry%determination%trace elements
采用加热消解处理样品，建立原子荧光法测定桑树不同部位Cu、Pb、Zn、Ni、Cd、Cr、Fe、Mn、Mg、K、Na和Ca 12种元素质量浓度的分析方法，采用ICP-AES测定样品中的微量元素。结果各种元素在其线性范围内线性关系良好，r在0.9995～0.9999之间，平均回收率在90.%～96.4%之间，RSD<3%（n=6），符合微量分析要求。本法简便，结果准确，重现性好，ICP-AES可同时测定多种元素，方便快捷。
採用加熱消解處理樣品，建立原子熒光法測定桑樹不同部位Cu、Pb、Zn、Ni、Cd、Cr、Fe、Mn、Mg、K、Na和Ca 12種元素質量濃度的分析方法，採用ICP-AES測定樣品中的微量元素。結果各種元素在其線性範圍內線性關繫良好，r在0.9995～0.9999之間，平均迴收率在90.%～96.4%之間，RSD<3%（n=6），符閤微量分析要求。本法簡便，結果準確，重現性好，ICP-AES可同時測定多種元素，方便快捷。
채용가열소해처리양품，건립원자형광법측정상수불동부위Cu、Pb、Zn、Ni、Cd、Cr、Fe、Mn、Mg、K、Na화Ca 12충원소질량농도적분석방법，채용ICP-AES측정양품중적미량원소。결과각충원소재기선성범위내선성관계량호，r재0.9995～0.9999지간，평균회수솔재90.%～96.4%지간，RSD<3%（n=6），부합미량분석요구。본법간편，결과준학，중현성호，ICP-AES가동시측정다충원소，방편쾌첩。
To establish a hydride generation-atomic fluorescence spectrometry to measure the content in different parts of mulberry by Cu,Pb,Zn,Ni,Cd,Cr,Fe,Mn,Mg,K,Na,Ca twelve trace elements with heat digestion. Concentrations of elements were determined by ICP-AES. Experimental results showed that linear relationship was good, r was between 0.999 5 and 0.999 9. Average recovery rate was between 90.0%and 96.4%, RSD was less than 3%(n=6). The results met requirement of microanalysis. The method proved to be simple , convenient and precise and can be used for control of ICP-AES method was rapid , accurate and convenient, can be used to determine various trace elements.
