粮油食品科技
糧油食品科技
량유식품과기
Science and Technology of Cereals, Oils and Foods
2015年
5期
72-76
,共5页
张东%薛雅琳%朱琳%柴杰
張東%薛雅琳%硃琳%柴傑
장동%설아림%주림%시걸
甘油三酯%三饱和脂肪酸甘油酯%液质联用%主成分分析
甘油三酯%三飽和脂肪痠甘油酯%液質聯用%主成分分析
감유삼지%삼포화지방산감유지%액질련용%주성분분석
triglyceride(TG)%trisaturated glyceride%high -performance liquid chromatography/quadru-pole -time of flying mass spectrometry(HPLC -Q /TOF)%principal component analysis
采用高效液相色谱—飞行时间质谱法对比分析棕榈油、猪脂、牛脂和羊脂甘油三酯,结果显示4种油脂的甘油三酯种类和含量均不相同。从棕榈油、猪脂、牛脂和羊脂分别鉴定出16、19、15、13种甘油三酯,三饱和脂肪酸甘油酯分别占9.13%、1.46%、13.75%及9.05%。棕榈油中 PPO 含量最高,占34.41%,其次是 PLO +SLL、PPL 和 PPP。猪脂中含量较高的甘油三酯分别为 OLS、PLO+SLL、POS 及 POO,占总甘油三酯的67.65%;牛脂中含量较大的甘油三酯为 POS 和 OLS,占40.17%,其次为 PPO、SSL 及 SOS;羊脂中含量较大的甘油三酯为 SSL、POO、SOS 和 POS,占73.12%。同时,采用主成分分析法对4种油脂进行了统计分析。
採用高效液相色譜—飛行時間質譜法對比分析棕櫚油、豬脂、牛脂和羊脂甘油三酯,結果顯示4種油脂的甘油三酯種類和含量均不相同。從棕櫚油、豬脂、牛脂和羊脂分彆鑒定齣16、19、15、13種甘油三酯,三飽和脂肪痠甘油酯分彆佔9.13%、1.46%、13.75%及9.05%。棕櫚油中 PPO 含量最高,佔34.41%,其次是 PLO +SLL、PPL 和 PPP。豬脂中含量較高的甘油三酯分彆為 OLS、PLO+SLL、POS 及 POO,佔總甘油三酯的67.65%;牛脂中含量較大的甘油三酯為 POS 和 OLS,佔40.17%,其次為 PPO、SSL 及 SOS;羊脂中含量較大的甘油三酯為 SSL、POO、SOS 和 POS,佔73.12%。同時,採用主成分分析法對4種油脂進行瞭統計分析。
채용고효액상색보—비행시간질보법대비분석종려유、저지、우지화양지감유삼지,결과현시4충유지적감유삼지충류화함량균불상동。종종려유、저지、우지화양지분별감정출16、19、15、13충감유삼지,삼포화지방산감유지분별점9.13%、1.46%、13.75%급9.05%。종려유중 PPO 함량최고,점34.41%,기차시 PLO +SLL、PPL 화 PPP。저지중함량교고적감유삼지분별위 OLS、PLO+SLL、POS 급 POO,점총감유삼지적67.65%;우지중함량교대적감유삼지위 POS 화 OLS,점40.17%,기차위 PPO、SSL 급 SOS;양지중함량교대적감유삼지위 SSL、POO、SOS 화 POS,점73.12%。동시,채용주성분분석법대4충유지진행료통계분석。
Triglycerides in palm oil and animal fats such as lard,beef tallow and suet were investigated by HPLC /Q -TOF.The results showed that the composition and content of triglycerides in each oil or fat were different.16,19,15 and 13 triglycerides were identified in palm oil,lard,beef tallow and suet,respec-tively;in which the content of trisaturated glycerides were 9.13%,1.46%,13.75% and 9.05%,sepa-rately.PPO was the major triglyceride (34.41%)in palm oil,followed by PLO +SLL,PPL and PPP. OLS,PLO +SLL,POS and POO with content of 67.65% were the dominant triglycerides in lard.In beef tallow,the content of POS and OLS was 40.17%,the content of PPO、SSL and SOS was relatively high. SSL、POO、SOS and POS in suet was 73.12%.Meanwhile,4 oils and fats were statistically analyzed u-sing principal component analysis (PCA).