中国处方药
中國處方藥
중국처방약
Journal Of China Prescription Drug
2015年
10期
26-27
,共2页
付瑾%王贝贝%赵爽%董洁%冀娇娇%刘永刚
付瑾%王貝貝%趙爽%董潔%冀嬌嬌%劉永剛
부근%왕패패%조상%동길%기교교%류영강
驱虫斑鸠菊%绿原酸%高效液相色谱法
驅蟲斑鳩菊%綠原痠%高效液相色譜法
구충반구국%록원산%고효액상색보법
Vernonia anthelmintica Willd%Chlorogenic acid%HPLC
目的 建立民族药驱虫斑鸠菊的质量标准,测定驱虫斑鸠菊中绿原酸的含量.方法 采用HPLC进行测定,以乙腈-0.4%磷酸(10:90)为流动相, 紫外检测波长为327 nm.结果 本法所采用的绿原酸的含量测定线性范围为0.06~1.2μg.平均回收率为100.78%,RSD为1.78%(n=6).结论 本文所建立的方法简便、灵敏、专属性强,为民族药驱虫斑鸠菊的质量评价提供了有效的方法.
目的 建立民族藥驅蟲斑鳩菊的質量標準,測定驅蟲斑鳩菊中綠原痠的含量.方法 採用HPLC進行測定,以乙腈-0.4%燐痠(10:90)為流動相, 紫外檢測波長為327 nm.結果 本法所採用的綠原痠的含量測定線性範圍為0.06~1.2μg.平均迴收率為100.78%,RSD為1.78%(n=6).結論 本文所建立的方法簡便、靈敏、專屬性彊,為民族藥驅蟲斑鳩菊的質量評價提供瞭有效的方法.
목적 건립민족약구충반구국적질량표준,측정구충반구국중록원산적함량.방법 채용HPLC진행측정,이을정-0.4%린산(10:90)위류동상, 자외검측파장위327 nm.결과 본법소채용적록원산적함량측정선성범위위0.06~1.2μg.평균회수솔위100.78%,RSD위1.78%(n=6).결론 본문소건립적방법간편、령민、전속성강,위민족약구충반구국적질량평개제공료유효적방법.
Objective To establish the quality standard for the Vernonia anthelmintica Willd.Methods Chlorogenic acid of the Vernonia anthelmintica Willd was determined by HPLC. The chromatographic conditions were: The mobile phase was methyl Cyanides-0.4%phosphoric acid(10:90), detection wave length of UV was 327 nm.Results The linear range of chlorogenic acid is 0.06~1.2μg . The average recovery was 100.78%,RSD was 1.78%(n=6).Conclusions The method was convenient,sensitive accurate and exclusive. It can control the quality of the Vernonia anthelmintica Willd.
