中国医药科学
中國醫藥科學
중국의약과학
China Medicine and Pharmacy
2015年
17期
57-60
,共4页
翟清%杨志伟%石鑫磊%范纯玲
翟清%楊誌偉%石鑫磊%範純玲
적청%양지위%석흠뢰%범순령
姜黄%金胺O%TLC%HPLC-MS法
薑黃%金胺O%TLC%HPLC-MS法
강황%금알O%TLC%HPLC-MS법
Turmeric%Auramine O%TLC%HPLC-MS
目的 建立姜黄用工业染料金胺O非法染色的检查方法.方法采用TLC法、HPLC-PAD法、HPLC-MS法,对多批次姜黄样品进行定性定量分析.结果 经检测30批市售样品中,有18批检出金胺,其质量浓度在0.12~0.86mg/g.结论 姜黄染色所用化工原料为金胺O,本研究所建立的检测方法,可以满足定性定量的要求.
目的 建立薑黃用工業染料金胺O非法染色的檢查方法.方法採用TLC法、HPLC-PAD法、HPLC-MS法,對多批次薑黃樣品進行定性定量分析.結果 經檢測30批市售樣品中,有18批檢齣金胺,其質量濃度在0.12~0.86mg/g.結論 薑黃染色所用化工原料為金胺O,本研究所建立的檢測方法,可以滿足定性定量的要求.
목적 건립강황용공업염료금알O비법염색적검사방법.방법채용TLC법、HPLC-PAD법、HPLC-MS법,대다비차강황양품진행정성정량분석.결과 경검측30비시수양품중,유18비검출금알,기질량농도재0.12~0.86mg/g.결론 강황염색소용화공원료위금알O,본연구소건립적검측방법,가이만족정성정량적요구.
Objective Establishment of turmeric with industrial dye staining auramine O illegal screening method.Methods The technique of TLC,HPLC-PAD and HPLC-MS were developed for qualitation and quantitative analysis mutiple batches of samples turmeric.ResultsAfter testing 30 batches of commercial samples,six batches detected in auramine,its content in the 0.12~0.86mg/g.Conclusion Turmeric staining with chemical raw materials for auramine O,detection method established in this paper,to meet with qualitative and quantitative requirements.
