广州化工
廣州化工
엄주화공
Guangzhou Chemical Industry
2015年
21期
78-79,138
,共3页
杨欢%黄小梅%邓祥%吴狄%李红琼%郭开雨%罗琼
楊歡%黃小梅%鄧祥%吳狄%李紅瓊%郭開雨%囉瓊
양환%황소매%산상%오적%리홍경%곽개우%라경
仙人掌%水热法%荧光碳量子点
仙人掌%水熱法%熒光碳量子點
선인장%수열법%형광탄양자점
cactus%hydrothermal method%fluorescent carbon dots
以仙人掌为碳源,通过水热法合成了荧光碳量子点,并通过荧光光谱对样品的光学性能进行了表征,同时考察了仙人掌用量、水热反应时间和温度对合成荧光碳量子点的影响。结果显示:以仙人掌为碳源合成的荧光碳量子点在水溶剂30 mL条件下,仙人掌质量为0.5 g时得到的荧光碳量子点发光效率最高;同时,水热反应时间为3 h,反应温度为160℃时得到的荧光碳量子点发光强度最高。荧光碳量子点在紫外灯照射下发出明亮的绿光。
以仙人掌為碳源,通過水熱法閤成瞭熒光碳量子點,併通過熒光光譜對樣品的光學性能進行瞭錶徵,同時攷察瞭仙人掌用量、水熱反應時間和溫度對閤成熒光碳量子點的影響。結果顯示:以仙人掌為碳源閤成的熒光碳量子點在水溶劑30 mL條件下,仙人掌質量為0.5 g時得到的熒光碳量子點髮光效率最高;同時,水熱反應時間為3 h,反應溫度為160℃時得到的熒光碳量子點髮光彊度最高。熒光碳量子點在紫外燈照射下髮齣明亮的綠光。
이선인장위탄원,통과수열법합성료형광탄양자점,병통과형광광보대양품적광학성능진행료표정,동시고찰료선인장용량、수열반응시간화온도대합성형광탄양자점적영향。결과현시:이선인장위탄원합성적형광탄양자점재수용제30 mL조건하,선인장질량위0.5 g시득도적형광탄양자점발광효솔최고;동시,수열반응시간위3 h,반응온도위160℃시득도적형광탄양자점발광강도최고。형광탄양자점재자외등조사하발출명량적록광。
Fluorescent carbon dots utilizing cactus as a carbon source via hydrothermal method was developed. Fluorescent carbon dots were characterized by fluorescence spectroscopy. The effect of the amount of cactus, reaction time and reaction temperature on hydrothermal synthesis process was investigated in the present work. The results indicated that when the total volume of the solvent water was 30 mL, 0. 5 g of cactus used was optimal because the obtained fluorescent carbon dots showed the highest luminescent efficiency. Besides, the optimized reaction time and temperature were set at 3 h and 160 ℃ owing to fluorescent carbon dots with the highest fluorescent intensities. The fluorescent carbon dots can emit bright green photoluminescence under UV excitation.