CAJ | 학술논문

采用索氏提取法（SE），同时蒸馏萃取法（SDE）和顶空固相微萃取法（HS －SPME）提取花锚不同部位（根、茎、叶、花）的挥发性成分，并运用 GC －MS 技术对所提取到的挥发性成分进行分析，同时结合 NIST2012谱图库检索出其主要化学成分。分析结果表明，采用3种不同提取方法从花锚的根、茎、叶、花4个不同部位共分离得到69个挥发性成分。采用同一方法提取不同部位得到的主要挥发性成分大致相似，主要差异表现在含量上。不同方法提取的主要挥发性成分略有差异，SE 法和 SDE 法提取的花锚不同部位的主要挥发性成分大致相同，主要是苯类、芥酸酰胺、酯类、酮类等，但其含量相差较大，而 HS －SPME 法提取的花锚不同部位的主要挥发性成分与 SE、SDE 法提取的挥发性成分存在明显差异，主要是醛类、酸类、酮类等。
채용색씨제취법（SE），동시증류췌취법（SDE）화정공고상미췌취법（HS －SPME）제취화묘불동부위（근、경、협、화）적휘발성성분，병운용 GC －MS 기술대소제취도적휘발성성분진행분석，동시결합 NIST2012보도고검색출기주요화학성분。분석결과표명，채용3충불동제취방법종화묘적근、경、협、화4개불동부위공분리득도69개휘발성성분。채용동일방법제취불동부위득도적주요휘발성성분대치상사，주요차이표현재함량상。불동방법제취적주요휘발성성분략유차이，SE 법화 SDE 법제취적화묘불동부위적주요휘발성성분대치상동，주요시분류、개산선알、지류、동류등，단기함량상차교대，이 HS －SPME 법제취적화묘불동부위적주요휘발성성분여 SE、SDE 법제취적휘발성성분존재명현차이，주요시철류、산류、동류등。
Using SE,SDE,HS -SPME extraction methods as well as GC -MS technique plus NIST2012 spectral library,the different chemical constituents of the volatile oils extracted from different parts (flowers,stems,leaves and roots)of Halenia corniculata were analyzed.Sixty-nine compounds were extracted from the flowers,stems,leav-es and roots of Halenia corniculata.The major volatile components including benzene,erucic acid amide,ester,ke-tone,etc.were roughly the same by SE and SDE methods,however,the contents of these chemical compositions were different.Compared with the above methods,the main volatile components extracted by HS -SPME method were significantly different,which were aldehydes,acids,ketones and so on.The results showed that the main vola-tile components were similar extracted from the roots,stems,leaves and flowers by the same extraction method but there were still individual differences.For example,the volatile constituents extracted from the flowers,stems,leaves and roots of Halenia corniculata using HS -SPME method were similar and the major differences were the relative content.