CAJ | 학술논문

在聚羧酸减水剂聚醚单体的合成过程中，催化剂的配制起到至关重要的作用。选择不同工段（设备）考察配置温度、配置压力、搅拌时间等因素对催化剂配制效果的影响。实验结果表明，在与 AB-10醇配置过程中，选择 V110罐进行配置 ZD-10催化剂，优化的配置浓度为0．8‰，配制温度30～40℃，循环温度90～96℃，HV145开度为50％，循环时间40 min；在与 OXAB-10中间体配置过程，选择 R103B 进行配置 ZD-10催化剂，使用 V101罐计量中间体量，则优化的配置浓度为0．6‰，配制温度60～70℃，搅拌时间40～50 min。
재취최산감수제취미단체적합성과정중，최화제적배제기도지관중요적작용。선택불동공단（설비）고찰배치온도、배치압력、교반시간등인소대최화제배제효과적영향。실험결과표명，재여 AB-10순배치과정중，선택 V110관진행배치 ZD-10최화제，우화적배치농도위0．8‰，배제온도30～40℃，순배온도90～96℃，HV145개도위50％，순배시간40 min；재여 OXAB-10중간체배치과정，선택 R103B 진행배치 ZD-10최화제，사용 V101관계량중간체량，칙우화적배치농도위0．6‰，배제온도60～70℃，교반시간40～50 min。
in the process of synthesis of polyether monomer,catalyst preparation plays a vital role. Different sections(equipment)to study the impact of temperature profiles,equipped with a pressure, stirring time and other factors of catalyst preparation effect.The experimental results show that the in and AB-10 alcohol in the configuration process,select v110 tank configuration ZD-10 catalyst, optimize configuration concentration is 0.8 per thousand,compounding temperature 30 ~ 40 ℃, temperature cycling 90 ~96 ℃,HV145 opening is 50%,the cycle time of 40 min;and OXAB-10 intermediate configuration process,choose R103B of configuration ZD-10 catalyst,using V101 metering tank intermediate volume,optimizing configuration concentration was 0.6 per thousand, compounding temperature 60 to 70 ℃,stirring time 40-50 min.