CAJ | 학술논문

亚麻柔软剂的优劣，直接影响亚麻制品的舒适性。本文针对当前氨基硅油和聚醚硅油在应用中存在的不足，利用本体聚合法，将聚醚、亚氨基基团链接至含氢硅油上，制备出新型有机硅亚麻柔软剂。实验分析了影响合成反应的因素，确定了合成的最佳条件为：合成温度为100℃，合成时间为8h，物料配比为含氢硅油∶双烯丙基聚醚∶N,N-亚甲基双丙烯酰胺=1.5∶1∶1，0.5mg·kg-1的催化剂（氯铂酸异丙醇混合溶液）使用量。合成的新型有机硅亚麻柔软剂，经红外光谱（FTIR）分析、核磁共振谱（H-NMR）分析、热性能（TG-DTA）分析等方法验证，能适合亚麻制品加工的需要。
아마유연제적우렬，직접영향아마제품적서괄성。본문침대당전안기규유화취미규유재응용중존재적불족，이용본체취합법，장취미、아안기기단련접지함경규유상，제비출신형유궤규아마유연제。실험분석료영향합성반응적인소，학정료합성적최가조건위：합성온도위100℃，합성시간위8h，물료배비위함경규유∶쌍희병기취미∶N,N-아갑기쌍병희선알=1.5∶1∶1，0.5mg·kg-1적최화제（록박산이병순혼합용액）사용량。합성적신형유궤규아마유연제，경홍외광보（FTIR）분석、핵자공진보（H-NMR）분석、열성능（TG-DTA）분석등방법험증，능괄합아마제품가공적수요。
The quality of the flax softener has a very important influence on the comfort of linen.The article is based on the current problems in the application of amino silicone oil and polyether silicone oil,In the experiment, the noumenon polymeric method was used to synthesize polyether and amino groups to the hydrogen containing sil-icone oil. A new type of flax softener was prepared.The factors affecting the synthesis reaction were analyzed,The optimum conditions for the synthesis were determined:the synthesis temperature is 100℃, the synthesis time is 8h, material ratio is hydrogen-containing silicone oil:double allyl polyether∶N,N-methylene-bis-acrylamide=1.5∶1∶1,0.5mg·kg-1 catalyst.The method was verified by infrared spectroscopy (FTIR)analysis, nuclear magnetic reso-nance spectroscopy(H-NMR)analysis and thermal performance(TG-DTA)analysis,the new type of flax softener is suitable for processing of linen.