陕西中医
陝西中醫
협서중의
Shaanxi Journal of Traditional Chinese Medicine
2015年
11期
1540-1544
,共5页
雷建林%杨翠%李芳%穆旭凯%车晓侠%李红
雷建林%楊翠%李芳%穆旭凱%車曉俠%李紅
뢰건림%양취%리방%목욱개%차효협%리홍
夏天无%原阿片碱%巴马汀%色谱法,高压液相%正交试验
夏天無%原阿片堿%巴馬汀%色譜法,高壓液相%正交試驗
하천무%원아편감%파마정%색보법,고압액상%정교시험
Corydalis decumbens%Protopine%Palmatine%Chromatography,high performance liquid%Or-thogonal test
目的：：优选夏天无醋炙最佳炮制工艺,为阐明醋炙入肝增效理论的科学性提供实验依据。方法：以高效液相色谱法测定夏天无及其炮制品中原阿片碱、盐酸巴马汀两个药效成分含量为衡量指标,采用正交试验设计优选夏天无炮制工艺。结果：加米醋量20%,浸润夏天无药材3h,中火130℃炒制5min为最佳炮制工艺。结论：优选的醋炙工艺稳定可行,能够较好地提高药效成分含量,醋用量、浸润时间、炒制温度对夏天无中有效成分溶出均有显著影响。
目的：：優選夏天無醋炙最佳砲製工藝,為闡明醋炙入肝增效理論的科學性提供實驗依據。方法：以高效液相色譜法測定夏天無及其砲製品中原阿片堿、鹽痠巴馬汀兩箇藥效成分含量為衡量指標,採用正交試驗設計優選夏天無砲製工藝。結果：加米醋量20%,浸潤夏天無藥材3h,中火130℃炒製5min為最佳砲製工藝。結論：優選的醋炙工藝穩定可行,能夠較好地提高藥效成分含量,醋用量、浸潤時間、炒製溫度對夏天無中有效成分溶齣均有顯著影響。
목적：：우선하천무작자최가포제공예,위천명작자입간증효이론적과학성제공실험의거。방법：이고효액상색보법측정하천무급기포제품중원아편감、염산파마정량개약효성분함량위형량지표,채용정교시험설계우선하천무포제공예。결과：가미작량20%,침윤하천무약재3h,중화130℃초제5min위최가포제공예。결론：우선적작자공예은정가행,능구교호지제고약효성분함량,작용량、침윤시간、초제온도대하천무중유효성분용출균유현저영향。
Obj ective :To select the best processing vinegar and processing methods of Corydalis decumbens. To provide the experimental basis for the scientific clarify vinegar into the liver of synergistic.Methods:HPLC was ap-plied to determine the content of protopine and palmatine from processed Corydalis decumbens and the processing was de-signed by orthogonal design.Results:The best sample was stir-frying at 130℃ for 5 min after adding 20% rice vinegar in-filtration 3hr.Conclusion:This optimum technology is stable and feasible,it can increase the contents of effective compo-nents better.The dosage of rice vinegar,time of vinegar infiltration,processing temperature are the main factors which af-fect markedly the quality of processed Corydalis decumbens stir-frying with vinegar.
