CAJ | 학술논문

利用顶空-气相色谱/质谱法分析了不同温度下典型电加热新型卷烟烟草材料和传统卷烟烟丝的挥发性成分.结果表明:①新型卷烟烟草材料和传统卷烟在不同温度段检测到的挥发性成分的数量不同;在200℃检测到的烟气挥发性成分最多,分别为67和82种.②检测到的挥发性成分主要为甲酸、乙酸、羟基丙酮、丙二醇、吡啶、糠醛、3-甲基戊酸、2,5-二甲基吡嗪、2(5H)-呋喃酮、甘油、烟碱等.其中新型卷烟烟气中甘油、丙二醇的释放量远远高于传统卷烟,传统卷烟烟气中挥发性吡嗪和呋喃酮类的释放量相对较高.③新型卷烟烟草材料典型挥发性成分的释放量随温度的升高先增大后减小,部分成分的释放量在120℃达到最大,部分成分在150℃达到最大.
이용정공-기상색보/질보법분석료불동온도하전형전가열신형권연연초재료화전통권연연사적휘발성성분.결과표명:①신형권연연초재료화전통권연재불동온도단검측도적휘발성성분적수량불동;재200℃검측도적연기휘발성성분최다,분별위67화82충.②검측도적휘발성성분주요위갑산、을산、간기병동、병이순、필정、강철、3-갑기무산、2,5-이갑기필진、2(5H)-부남동、감유、연감등.기중신형권연연기중감유、병이순적석방량원원고우전통권연,전통권연연기중휘발성필진화부남동류적석방량상대교고.③신형권연연초재료전형휘발성성분적석방량수온도적승고선증대후감소,부분성분적석방량재120℃체도최대,부분성분재150℃체도최대.
The volatile components in tobacco material of typical electric heating type cigarette and cut filler in traditional cigarette released at different temperatures were analyzed by headspace-gas chromatography-mass spectrometry (HS-GC/MS). The results showed that: 1) The numbers of detectable volatile components released from tobacco material of novel cigarette and traditional cigarette differed and reached their maxima 67 and 82, respectively, at 200 ℃. 2) The main detected volatile components included formic acid, acetic acid, hydroxyacetone, propylene glycol, pyridine, furfural, 3-methylvaleric acid, 2,5-dimethylpyrazine, 2(5H)-furanone, glycerol, nicotine. The novel cigarette released much more glycerol and propylene glycol than did traditional cigarette, while traditional cigarette released more volatile pyrazines and furanones. 3)The typical volatile components released by novel cigarette increased first then decreased with the rise of temperature, some of them peaked at 120 ℃ and some at 150 ℃.