CAJ | 학술논문

目的：建立牛黄镇惊丸中牛黄含量测定的检测方法。方法采用高效液相色谱法测定牛黄中胆红素的含量。结果胆红素在0.009968～0.4984μg范围内，,进样量与峰面积线性关系良好（r=0.9999）；平均加样回收率98.4%（R S D=0.9%）。结论该方法操作简便、结果准确、重现性好，可用于牛黄镇惊丸中牛黄的含量测定。
목적：건립우황진량환중우황함량측정적검측방법。방법채용고효액상색보법측정우황중담홍소적함량。결과담홍소재0.009968～0.4984μg범위내，,진양량여봉면적선성관계량호（r=0.9999）；평균가양회수솔98.4%（R S D=0.9%）。결론해방법조작간편、결과준학、중현성호，가용우우황진량환중우황적함량측정。
Objective :To establish an method for the determination of calculus bovis in Niuhuang Zhen Jing pil . Methods: HPLC analysis was used to determine the content of bilirubin in calculus bovis . Results: This method had good linearity in the range of 0.009968~0.4984μg(r=0.9999);The average recovery was 98.4%(RSD=0.9%).Conclusion: The method was shown to be convenient, accurate with good repeatability, so it was suitable to determine the content of Calculus bovis in Niu huang Zhen Jing pil .