CAJ | 학술논문

建立银丹心脑通软胶囊中挥发性成分冰片的含量测定方法。色谱柱：30m×0.25um×0.32mm，填料为聚乙二醇。进样口温度160℃，柱温140℃，检测器温度180℃，检测器为FID检测器，载气为氮气，分流比为50：1，进样量1uL，理论板数按龙脑峰计算应不低于5000。乙酸乙酯为溶剂，水杨酸甲酯为内标。龙脑在0.17469mg/mL到1.7468mg/mL的浓度范围内峰面积比与浓度呈良好线性关系（R2=0.9999），平均回收率为98.1%，RSD%为0.87%。该法快速、灵敏、准确、可靠，可作为银丹心脑通软胶囊质量评价的依据。
건립은단심뇌통연효낭중휘발성성분빙편적함량측정방법。색보주：30m×0.25um×0.32mm，전료위취을이순。진양구온도160℃，주온140℃，검측기온도180℃，검측기위FID검측기，재기위담기，분류비위50：1，진양량1uL，이론판수안용뇌봉계산응불저우5000。을산을지위용제，수양산갑지위내표。용뇌재0.17469mg/mL도1.7468mg/mL적농도범위내봉면적비여농도정량호선성관계（R2=0.9999），평균회수솔위98.1%，RSD%위0.87%。해법쾌속、령민、준학、가고，가작위은단심뇌통연효낭질량평개적의거。
Dan-SIM established silver thong in soft capsule of brain volatiles content determination method of Borneol. Chromatographic columns: 30m×0.25um×0.32mm, fil ers to polyethylene glycol. Injector temperature 160 ° C, column temperature of 140 ° C, temperature 180 ° C detector, detector FID detector carrier gas nitrogen gas, split ratio is 50:1, the sample size 1uL, theoretical plate number calculated by Dragon head peak should not be less than 5000. Ethyl acetate as a solvent, methyl ester salicylic acid as internal standard. Borneol within the concentration range of 0.17469mg/mL to 1.7468mg/ml is a good linear correlation between peak area ratio and concentration (R2=0.9999), with an average recovery rate of 97.3%, RSD 0.5. This method is fast, responsive, accurate, reliable, and can serve as a silver Dan-SIM based on quality evaluation of effect of soft capsule of the brain.