华西药学杂志
華西藥學雜誌
화서약학잡지
WEST CHINA JOURNAL OF PHARMACEUTICAL SCIENCES
2001年
1期
54-55
,共2页
麻黄%肉桂%三棱%盐酸麻黄碱%薄层色谱扫描%活骨颗粒
痳黃%肉桂%三稜%鹽痠痳黃堿%薄層色譜掃描%活骨顆粒
마황%육계%삼릉%염산마황감%박층색보소묘%활골과립
目的：建立活骨颗粒中麻黄、肉桂、三棱TLC鉴别及测定盐酸麻黄碱含量的方法。方法：采用薄层色谱和薄层扫描法。结果：线性范围0.5～3.0 μg，回收率97.83%。RSD为3.32%。结论：该法准确，重复性好，适用于制剂的含量测定。
目的：建立活骨顆粒中痳黃、肉桂、三稜TLC鑒彆及測定鹽痠痳黃堿含量的方法。方法：採用薄層色譜和薄層掃描法。結果：線性範圍0.5～3.0 μg，迴收率97.83%。RSD為3.32%。結論：該法準確，重複性好，適用于製劑的含量測定。
목적：건립활골과립중마황、육계、삼릉TLC감별급측정염산마황감함량적방법。방법：채용박층색보화박층소묘법。결과：선성범위0.5～3.0 μg，회수솔97.83%。RSD위3.32%。결론：해법준학，중복성호，괄용우제제적함량측정。
OBJECTIVE:TLC and TLC-scanning method were used to identify Herb ephedrae， Cortex cinnamomi，Rhizoma sparganii and to determine the ephedrine hydrochloride in Huogu granules.METHODS:To use TLC and TLC-scanning method.RESULTS:Calibration curve was linearity within the range of 0.5～3.0 μg（r =0.9990）, the average was 97.83% , and RSD was 3.32%.CONCLUSION:The method was sensitive , accurate and rapid , it is suitable for quantitative determination .
