分析化学
分析化學
분석화학
CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
2001年
3期
333-335
,共3页
李世凤%崔华%孙玉刚%林祥钦
李世鳳%崔華%孫玉剛%林祥欽
리세봉%최화%손옥강%림상흠
鲁米诺%单宁酸%流动注射%化学发光增强
魯米諾%單寧痠%流動註射%化學髮光增彊
로미낙%단저산%류동주사%화학발광증강
发现单宁酸对Luminol-KIO4-Mn2+碱性体系的化学发光有较强增敏作用,据此建立了流动注射化学发光增强法测定单宁酸的新方法。该法简单、快速、线性范围宽,测定单宁酸的检出限为9×10-9 mol/L;线性范围为3×10-8~5×10-6 mol/L,对于1×10-6 mol/L单宁酸测定的相对标准偏差1.5%(n=11)。应用于五倍子中单宁酸的测定,结果满意
髮現單寧痠對Luminol-KIO4-Mn2+堿性體繫的化學髮光有較彊增敏作用,據此建立瞭流動註射化學髮光增彊法測定單寧痠的新方法。該法簡單、快速、線性範圍寬,測定單寧痠的檢齣限為9×10-9 mol/L;線性範圍為3×10-8~5×10-6 mol/L,對于1×10-6 mol/L單寧痠測定的相對標準偏差1.5%(n=11)。應用于五倍子中單寧痠的測定,結果滿意
발현단저산대Luminol-KIO4-Mn2+감성체계적화학발광유교강증민작용,거차건립료류동주사화학발광증강법측정단저산적신방법。해법간단、쾌속、선성범위관,측정단저산적검출한위9×10-9 mol/L;선성범위위3×10-8~5×10-6 mol/L,대우1×10-6 mol/L단저산측정적상대표준편차1.5%(n=11)。응용우오배자중단저산적측정,결과만의
A novel flow injection chemiluminescent enhancement method for the determination of tannic acid based on luminol-KIO4-Mn2+ system is developed. The method is simple, rapid and effective to determine tannic acid in the range of 3.0×10-8~5.0×10-6 mol/L with a detection limit of 9×10-9 mol/L. The relative standard deviation is 1.5% for the determination of 1.0×10-6 mol/L tannic acid (n=11). The mehtod has been applied to determine the content of tannic acid in Chinese gall with satisfactory results.