CAJ | 학술논문

用动态涂敷法制备了对甲苯磺酸正丁铵玻璃毛细管柱柱1(固定液浓度为7.5%，柱尺寸为35m×0.35mm i.d.)和柱2(固定液浓度为9.2%,柱尺寸为35m×0.30mm i.d.),所用溶剂是丙酮和甲醇(2∶1V／V)的混合溶剂,并对柱性能进行了考察。结果表明,这种色谱固定相具有较强的极性并对饱和烃、芳香烃、饱和酸、芳香酸、极性异构体等具有良好的分离效果。
용동태도부법제비료대갑분광산정정안파리모세관주주1(고정액농도위7.5%，주척촌위35m×0.35mm i.d.)화주2(고정액농도위9.2%,주척촌위35m×0.30mm i.d.),소용용제시병동화갑순(2∶1V／V)적혼합용제,병대주성능진행료고찰。결과표명,저충색보고정상구유교강적겁성병대포화경、방향경、포화산、방향산、겁성이구체등구유량호적분리효과。
Capillary gas chromatographic column 1 (7.5%　W/W,3 5×0. 35mm i.d.) and column 2 (9.2% W/W,35×0.30mm i.d.) using butylammonium 4-to unesulfonate as stationary phase were prepared by the method of dynamic coating with mercury plug, and the solvent used was mixture of acetone and methanol (2 ∶1　V/V). The results　showed that the column had good chromatograpic pro perties, especially to strong polar compound, such as carboxylic acids and acoho ls could be separated well.